1. Introduction Electrospinning is a technology that prepares polymer solution or melt into nanofibers through high voltage electric fields. In recent years, nanocellulose has become a hot material for electrospinning research due to its excellent mechanical properties, biocompatibility and degradability. Nanocellulose fibers prepared by electrospinning have broad application prospects in the fields of filtration, biomedicine, energy storage, etc. This article will introduce in detail the preparation process of nanocellulose electrospinning method. 2. Experimental materials: cellulose raw materials: microcrystalline cellulose (MCC), lignocellulose or bacterial cellulose (BC). Solvents: N,N-dimethylformamide (DMF), acetone, ethanol, ionic liquids (such as 1-ethyl-3-methylimidazole acetate, [EMIM][OAc]), etc. Additives: polyvinyl alcohol (PVA), polyethylene oxide (PEO), chitosan, etc., used to adjust the viscosity and electrospinning properties of the solution. Crosslinking agent: glutaraldehyde (G
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